CobaltMaghrebV1, France, Analysis, bibRecord, 000209

The T#2-Li2/3Co2/3Mn1/3O2 system. 1. Its structural characterization

Identifieur interne : 000209 ( France/Analysis ); précédent : 000208; suivant : 000210

The T#2-Li2/3Co2/3Mn1/3O2 system. 1. Its structural characterization

Auteurs : F. Tournadre [France] ; L. Croguennec [France] ; I. Saadoune [France, Maroc] ; F. Weill [France] ; Y. Shao-Horn [France, États-Unis] ; P. Willmann [France] ; C. Delmas [France]

Source :

Chemistry of materials [ 0897-4756 ] ; 2004.

RBID : Pascal:04-0530343

Descripteurs français

Pascal (Inist)
- Composé minéral, Composé organique, Polymère.
Wicri :
- topic : Composé minéral, Polymère.

English descriptors

KwdEn :
- Inorganic compounds, Organic compounds, Polymers.

Abstract

The layered T#2-Li_2/3Co_2/3Mn_1/3O₂ phase was obtained by ion exchange in molten salts of Na⁺ by Li⁺ in P2-Na_2/3Co_2/3Mn_1/3O₂. X-ray photoelectron spectroscopy (XPS) analyses have shown that cobalt and manganese ions are present in T#2-Li_2/3Co_2/3Mn_1/3O₂ at the trivalent and tetravalent oxidation states, respectively. The refinement of the neutron diffraction data was achieved, and the structure was described in the Cmca space group with two Co_2/3Mn_1/3O₂ slabs per unit cell. Thanks to nuclear density Fourier difference maps calculations, it was shown that the lithium ions are distributed in the 8e and 8f_edges tetrahedral sites. Transmission electron microscopy has shown no evidence of lithium ordering in the interslab space.

Affiliations:

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Le document en format XML

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Co<sub>2/3</sub>
Mn<sub>1/3</sub>
O<sub>2</sub>
 system. 1. Its structural characterization</title>
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<sourceDesc><biblStruct><analytic><title xml:lang="en" level="a">The T#2-Li<sub>2/3</sub>
Co<sub>2/3</sub>
Mn<sub>1/3</sub>
O<sub>2</sub>
 system. 1. Its structural characterization</title>
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<affiliation wicri:level="4"><inist:fA14 i1="01"><s1>Institut de Chimie de la Matière Condensée de Bordeaux-CNRS and Ecole Nationale Supérieure de Chimie et Physique de Bordeaux, Université Bordeaux I, 87 Au. du Dr A. Schweitzer</s1>
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<wicri:noRegion>Cambridge, Massachusetts 02139</wicri:noRegion>
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</author>
<author><name sortKey="Willmann, P" sort="Willmann, P" uniqKey="Willmann P" first="P." last="Willmann">P. Willmann</name>
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<s3>FRA</s3>
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<country>France</country>
<placeName><region type="region" nuts="2">Occitanie (région administrative)</region>
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<settlement type="city">Toulouse</settlement>
</placeName>
</affiliation>
</author>
<author><name sortKey="Delmas, C" sort="Delmas, C" uniqKey="Delmas C" first="C." last="Delmas">C. Delmas</name>
<affiliation wicri:level="4"><inist:fA14 i1="01"><s1>Institut de Chimie de la Matière Condensée de Bordeaux-CNRS and Ecole Nationale Supérieure de Chimie et Physique de Bordeaux, Université Bordeaux I, 87 Au. du Dr A. Schweitzer</s1>
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<placeName><region type="region" nuts="2">Nouvelle-Aquitaine</region>
<region type="old region" nuts="2">Aquitaine</region>
<settlement type="city">Pessac</settlement>
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<series><title level="j" type="main">Chemistry of materials</title>
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<term>Organic compounds</term>
<term>Polymers</term>
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<keywords scheme="Pascal" xml:lang="fr"><term>Composé minéral</term>
<term>Composé organique</term>
<term>Polymère</term>
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<front><div type="abstract" xml:lang="en">The layered T#2-Li<sub>2/3</sub>
Co<sub>2/3</sub>
Mn<sub>1/3</sub>
O<sub>2</sub>
 phase was obtained by ion exchange in molten salts of Na<sup>+</sup>
 by Li<sup>+</sup>
 in P2-Na<sub>2/3</sub>
Co<sub>2/3</sub>
Mn<sub>1/3</sub>
O<sub>2</sub>
. X-ray photoelectron spectroscopy (XPS) analyses have shown that cobalt and manganese ions are present in T#2-Li<sub>2/3</sub>
Co<sub>2/3</sub>
Mn<sub>1/3</sub>
O<sub>2</sub>
 at the trivalent and tetravalent oxidation states, respectively. The refinement of the neutron diffraction data was achieved, and the structure was described in the Cmca space group with two Co<sub>2/3</sub>
Mn<sub>1/3</sub>
O<sub>2</sub>
 slabs per unit cell. Thanks to nuclear density Fourier difference maps calculations, it was shown that the lithium ions are distributed in the 8e and 8f<sub>edges</sub>
 tetrahedral sites. Transmission electron microscopy has shown no evidence of lithium ordering in the interslab space.</div>
</front>
</TEI>
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<li>Maroc</li>
<li>États-Unis</li>
</country>
<region><li>Aquitaine</li>
<li>Marrakech-Tensift-Al Haouz</li>
<li>Midi-Pyrénées</li>
<li>Nouvelle-Aquitaine</li>
<li>Occitanie (région administrative)</li>
</region>
<settlement><li>Marrakech</li>
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<li>Toulouse</li>
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<orgName><li>Université Bordeaux I</li>
</orgName>
</list>
<tree><country name="France"><region name="Nouvelle-Aquitaine"><name sortKey="Tournadre, F" sort="Tournadre, F" uniqKey="Tournadre F" first="F." last="Tournadre">F. Tournadre</name>
</region>
<name sortKey="Croguennec, L" sort="Croguennec, L" uniqKey="Croguennec L" first="L." last="Croguennec">L. Croguennec</name>
<name sortKey="Delmas, C" sort="Delmas, C" uniqKey="Delmas C" first="C." last="Delmas">C. Delmas</name>
<name sortKey="Saadoune, I" sort="Saadoune, I" uniqKey="Saadoune I" first="I." last="Saadoune">I. Saadoune</name>
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<name sortKey="Weill, F" sort="Weill, F" uniqKey="Weill F" first="F." last="Weill">F. Weill</name>
<name sortKey="Willmann, P" sort="Willmann, P" uniqKey="Willmann P" first="P." last="Willmann">P. Willmann</name>
</country>
<country name="Maroc"><region name="Marrakech-Tensift-Al Haouz"><name sortKey="Saadoune, I" sort="Saadoune, I" uniqKey="Saadoune I" first="I." last="Saadoune">I. Saadoune</name>
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<country name="États-Unis"><noRegion><name sortKey="Shao Horn, Y" sort="Shao Horn, Y" uniqKey="Shao Horn Y" first="Y." last="Shao-Horn">Y. Shao-Horn</name>
</noRegion>
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</record>

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   |flux=    France
   |étape=   Analysis
   |type=    RBID
   |clé=     Pascal:04-0530343
   |texte=   The T#2-Li2/3Co2/3Mn1/3O2 system. 1. Its structural characterization
}}

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	Serveur d'exploration sur le cobalt au Maghreb
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Serveur d'exploration sur le cobalt au Maghreb

The T#2-Li2/3Co2/3Mn1/3O2 system. 1. Its structural characterization

The T#2-Li2/3Co2/3Mn1/3O2 system. 1. Its structural characterization

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